identification of fibre – Textile | chemwifi

 Fiber Analysis: Qualitative

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1 Fiber Analysis: Qualitative
identification of textile fibre- microscope

1. Grouped By Generic Classifications of Textile Fibres

Group 1 – Natural Fibers

   Natural Fibers

a.
Cellulose
(Vegetable)

b.
Keratin (Animal)

(Natural
Protein Fibres)

c.
Mineral

 1.
Seed Fibres

Cotton

Akund

Kapok

 

 1.
Wool & Chlorinated wool

 

·       
Asbestos

 

 

 2.
Silk

Bombyx
(cultivated)

Tasar
or Tussah (wild)

 

 

2.
Bast Fibres

 I. Low Lignin Content

Linen or Flax

Ramie

II. High Lignin Content

Jute

Mesta

Rosella

True Hemp

Sunn Hemp

 

3.

 Alpaca

Camel

Cashmere

Horse

llama

Mohair

Rabbit

Vicuna

Yak

 

3.
Leaf Fibres

Manila
Hemp (Abaca)

Sisal
(Agave)

 

4.
Fruit or Nut Fibre

Coir

 

Group 2 – Man-Made Fibers

   Man Made Fibers

a.
Regenerated Fibres

b.
Synthetic Fibres

 1.
Cellulosic

Viscose

Cuprammonium

Acetate
(secondary & triacetate)

Polynosic

High-Wet
Modulus Fibres (HWM)

 

 

 

 1.
Polyamides

Nylon
6

Nylon
66

Nylon
610

Etc…

 

 

 

 2.
Polyester

Terylene

Terene

Dacron

Etc…

 

 

 

2.
Protein

Casein

Groundnut
Fibre

Zein

 

 

 

 

 3.
Polyvinyl Derivatives

 I.
Polyvinyl
Chloride

Pe Ce

Rhovyl

Etc…

 II.
Polyvinyl
Chloride Acetate

Vinylon
ST

Vinyon
HH

 III.
Polyvinyl Chloride Acrylonitrile

Vinyon
N

Dynel

 IV.
Polyvinylonitrile
(Acrylic fibre)

Orlon

Acrilan

 V.
Polyvinyl
Alcohol

Vinylon

Kuralon

 VI.
Polystyrene
& Copolymers

Styroflex

Polyfil

Etc..

 VII.
Polyvinylidene Chloride & Copolymers

 Saran

Velon

 

 

 

 

 4.
Polyolefins

 I.
Polyethylene

Polythene

 II.
Polypropylene

Reevon

 

Group 3 – Inorganic Fibers

Inorganic Fibres
a. Glass
b. Metal

2. Fibre identification by Burning Test-

A small tuft of fibres is held by forceps in the frame of a micro-burner for about
10 seconds and is then removed. It is noted whether the tuft burns or not; whether it forms any bead or whether the ash skeleton is retained; the type of smell emitted during burning is also noted. The test is carried out in daylight. 

Fibre-identification-by-Burning-Test

Reaction to Flame

Reaction-to-flame-natural-fibres
Reaction-to-flame-man-made-fibres
Reaction-to-flame-inorganic-fibres

3. Fibre identification by Density

Identification Density & Melting
Point

Natural Fibre

Density g/cc

Melting Point ℃

Asbestos (chrysotile)

2.1-2.8

Over 350

Cellulose

1.51

none

Silk

1.32-1.34

none

Wool & Other Hair

1.15-1.30

none

Identification Density & Melting
Point

Man-Made Fibre

Density g/cc

Melting Point ℃

Acetate, Secondary

1.32

260

Acetate, tri

1.30

288

Acrylic

1.12-1.19

none

Anidex

1.22

Softens at 190℃

Aramid

1.38

Char at 400℃

Azlon

1.30

none

Modacrylic

1.30 or 1.36

188 or 120

Novoloid

1.25

none

Nylon

1.12-1.15

213-225

Nylon 6,6

1.12-1.15

256-265

Nytril

1.20

218

Polyester

1.38 or 1.23

250-260 or 282

Polyethylene

0.90-0.92

135

polypropylene

0.90-0.92

170

Rayon

1.51

none

Rubber

0.96-1.06

none

Saran

1.70

168

Spandex

1.20-1.21

230

Vinal

1.26-1.30

Vinyon

1.34-1.37

230 or 400

Identification Density & Melting
Point

Inorganic Fibre

Density g/cc

Melting Point ℃

Metallic

Varies

Over 300

Glass

2.4-2.6

850

4. Fibre identification by Solubility Test

fibre-identification-by-solubility-test

Floatation Test –

A small sample of the fibre after degreasing in benzene-methanol mixture ( 3:2 ) is placed in the test liquid and pushed below the surface by means of a glass rod. The liquid should be illuminated transversely and viewed against a black background to observe whether the sample floats on the surface or sinks.

5. Fibre identification by Microscope

Microscopic Analysis

Longitudinal Examination – Place a small number of fibres on a glass slide in a suitable
mounting medium, cover the fibres with a covering glass. Examine the fibres at a specified magnification under microscope.

Cross-Section Examination – Take a tuft of fibres and prepare the specimen with the
cross-sectioning device, place it on a glass slide in a suitable mounting medium and cover it with a covering glass. Examine the fibres at a specified magnification under microscope.


Photomicrographs of Common Textile Fibers

Cross-Section 500X - Cotton
Cross-Section 500X – Cotton fibre (not mercerized)
Longitudinal View-500X - Cotton fibre (mercerized)
Longitudinal View-500X – Cotton fibre (not mercerized)
Cross-Section 500X - Cotton

Cross-Section 500X – Cotton fibre (mercerized)

Longitudinal View-500X - Cotton fibre (mercerized)

Longitudinal View-500X – Cotton fibre (mercerized)

Cross-Section-500X-Flax-fibre

Cross-Section-500X Flax fibre

Longitudinal-View-500X-flax-fibre

Longitudinal-View-500X-Flax fibre

Cross-Section-500X hemp fibre

Cross-Section-500X- Hemp fibre

Longitudinal-View-500X-Hemp fibre

Longitudinal-View-500X-Hemp fibre

Cross-Section-500X-jute-fibre

Cross-Section-500X- Jute fibre

Longitudinal-View-500X-jute-fibre
Longitudinal-View-500X-jute-fibre
Cross-Section-500X-Ramie-fibre
Cross-Section-500X-Ramie fibre
Longitudinal-View-500X-Ramie-fibre

Longitudinal-View-500X-Ramie fibre

Cross-Section-500X-Sisal-fibre

Cross-Section-500X- Sisal fibre

Longitudinal-View-500X-Sisal-fibre

Longitudinal-View-500X-Sisal fibre

Cross-Section-500X-Abaca-fibre

Cross-Section-500X-Abaca fibre

Longitudinal-View-500X-Abaca-fibre
Longitudinal-View-500X-Abaca fibre
Cross-Section-500X-Kenaf-fibre
Cross-Section-500X-Kenaf-fibre
Longitudinal-View-500X-Kenaf-fibre

Longitudinal-View-500X-Kenaf-fibre

Cross-Section-500X-wool-fibre

Cross-Section-500X-Wool-fibre

Longitudinal-View-500X-Wool-fibre

Longitudinal-View-500X-Wool fibre

Cross-Section-500X-Mohair-fibre

Cross-Section-500X-Mohair fibre

Longitudinal-View-500X-Mohair-fibre
Longitudinal-View-500X-Mohair-fibre
Cross-Section-500X-Phormium-fibre

Cross-Section-500X-Phormium-fibre

Longitudinal-View-500X-phormium-fibre

Longitudinal-View-500X- Phormium fibre

Cross-Section-500X-Cashmere-fibre

Cross-Section-500X- Cashmere fibre

Longitudinal-View-500X-Cashmere-fibre

Longitudinal-View-240X- Cashmere fibre

SEM (Cashmere).

Longitudinal-View-1500X- Cashmere fibre

Cross-Section-500X-Camel hair

Cross-Section-500X-Camel hair

Longitudinal-View-500X-Camel-hair-fibre

Longitudinal-View-500X-Camel-hair-fibre

Cross-Section-500X-Silk-fibre

Cross-Section-500X-Silk-fibre

Longitudinal-View-500X-silk-fibre

Longitudinal-View-500X-silk-fibre

Cross-Section-500X-Silk-tussah-fibre

Cross-Section-500X-Silk-tussah-fibre

Longitudinal-View-500X-silk-tussah-fibre

Longitudinal-View-500X-silk-tussah-fibre

Cross-Section-500X-polyester-fibre

Cross-Section-500X- Polyester fibre

Longitudinal-View-250X-polyester-fibre

Longitudinal-View-250X-Polyester-fibre

REFFERENCE SPECIFICATION     :    IS 667: 1981 & AATCC 20- 2007

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